Hanna-instruments HI 903 Bedienungsanleitung Seite 129
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9-1
METHODS OPTIMIZATION
Chapter 9. Contents
9 OPTIMIZATION ..................................................................................... 9-3
9.1 Titrator Settings ................................................................................... 9-3
9.1.1 Control Parameters.................................................................................... 9-3
9.1.1.1 Endpoint Potential and Polarization Current ........................................................9-3
9.1.1.2 Dosing Parameters ..........................................................................................9-4
9.1.1.2.1 Minimum Dose ........................................................................................9-4
9.1.1.2.2 Maximum Dose .......................................................................................9-4
9.1.1.3 Timed Increment ............................................................................................9-5
9.1.1.4 Start Mode .....................................................................................................9-6
9.1.1.5 Signal Averaging ..............................................................................................9-6
9.1.1.6 Flow Rate .......................................................................................................9-6
9.1.2 Termination Parameters .............................................................................. 9-6
9.1.2.1 Stability Time ..................................................................................................9-6
9.1.2.2 Drift Stop Termination Criteria ...........................................................................9-6
9.1.2.2.1 Relative Drift Stop ...................................................................................9-7
9.1.2.2.2 Absolute Drift Stop ..................................................................................9-7
9.1.3 Method Options .......................................................................................... 9-8
9.1.3.1 Pre-Dispensing Amount ....................................................................................9-8
9.1.3.2 Pre-Analysis Stir Time ......................................................................................9-8
9.1.3.3 Stirring Speed..................................................................................................9-8
9.1.3.4 Background Drift Rate Entry.............................................................................9-8
9.2 The Sample ........................................................................................... 9-9
9.2.1 Proper Sampling Procedure ......................................................................... 9-9
9.2.2 Determining the Optimal Sample Size .......................................................... 9-9
9.2.3 Solid Samples............................................................................................. 9-10
- QUICK START GUIDE 1
- KARL FISCHER 1
- VOLUMETRIC TITRATOR 1
- INSTRUCTION MANUAL 19
- Dear customer 20
- © 2013 Hanna Instruments 20
- TABLE OF CONTENTS 21
- INTRODUCTION 23
- Chapter 2. Contents 25
- 2.1 Unpacking 27
- 2.2 Safety Measures 28
- 2.3 Installation 29
- 2.3.2 Titrator Rear View 30
- 2.3.3 Titrator Left-side View 30
- 2.3.4 Titrator Assembly 31
- 2.3.4.2 Attaching the Burette 33
- Karl Fischer Electrode 36
- Solvent Handling System 36
- Extension 37
- Caution: 39
- USER INTERFACE 41
- GENERAL OPTIONS 51
- Chapter 5. Contents 65
- 5 METHODS 67
- 5.2 Standard Methods 68
- 5.3 User Methods 69
- 5.4 View / Modify Method 70
- 5.5 Method Options 71
- 5.5.2 Method Revision 72
- 5.5.3 Method Type 72
- 5.5.4 Predispensing Amount 73
- 5.5.5 Pre-Analysis Stir Time 73
- 5.5.6 Stirring Speed 74
- 5.5.7 Stirbar Type 74
- 5.5.8 Drift Entry 75
- Sample Analysis 76
- External extraction 77
- External dissolution 77
- 4.11, Setup Balance Interface 78
- Titrant Standardization 79
- 5.5.13 Titrant 81
- 5.5.14 Control Parameters 83
- Cautious 84
- Standby Duration 84
- 1 Reading 87
- 5.5.15 Termination Parameters 88
- 5.5.14.4, End Point 90
- Stability Time) 90
- 5.6 Printing 91
- TITRATION 100
- AUXILIARY FUNCTIONS 107
- MAINTENANCE, PERIPHERALS 117
- METHODS OPTIMIZATION 129
- Appendix 1. Contents 147
- APPENDIX 1 148
- APPENDIX 2 151
- Appendix 3. Accessories 155
- APPENDIX 3 156
- GENERAL APPLICATIONS BROCHURE 161
- Results: 164
- Method ID: HI8104EN 178
- Method ID: HI8106EN 181
- Method ID: HI8107EN 183
- Method ID: HI8108EN 185
- Method ID: HI8301EN 192
- TITRATION THEORY 193
- Principles 193
- 5 CALCULATIONS 213
- 214
- 214
- 214
- 215
- 215
- 215
- By Volume 216
- 5.2.3 Blank Titration 216
- 5.2.5 Back Titration 217
- 6 GLOSSARY 218
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